2-Chloro-1,1,1,3-tetrafluoropropane

Base Information

• Chemical Name: 2-Chloro-1,1,1,3-tetrafluoropropane
• CAS No.: 117970-90-8
• Molecular Formula: C3H3 Cl F4
• Molecular Weight: 150.503
• Mol file: 117970-90-8.mol

Synonyms:1,1,1,3-Tetrafluoro-2-chloropropane;2-Chloro-1,1,1,3-tetrafluoropropane; HCFC 244db; HCFO 244db

Chemical Property of 2-Chloro-1,1,1,3-tetrafluoropropane

Chemical Property:

• Refractive Index: 1.3063 (estimate)
• Boiling Point: 11.95°C (rough estimate)
• PSA: 0.00000
• Density: 1.2432 (estimate)
• LogP: 2.12560

Purity/Quality:

99%min ^*data from raw suppliers

2-Chloro-1,1,1,3-tetrafluoropropane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Chloro-1,1,1,3-tetrafluoropropane

There total 12 articles about 2-Chloro-1,1,1,3-tetrafluoropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1,1,2,3-Tetrachloropropene (10436-39-2) → 2-chloro-1,1,1-trifluoropropene (2730-62-3) + 2-chloro-1,1,1,2-tetrafluoropropane (421-73-8) + 1,1,1,2,3-pentafluoropropane (431-31-2) + 2,3-dichloro-1,1,1-trifluoropropane (338-75-0) + 1-chloro-2,3,3,3-tetrafluoropropane (151771-09-4) + 2-chloro-1,3,3,3-tetrafluoropropane (117970-90-8)

Guidance literature:

With hydrogen fluoride; antimonypentachloride; at 100 - 125 ℃; for 12h; under 33082.7 - 39185.2 Torr; Product distribution / selectivity;

Reference yield:

1,1,1-trifluoropropylene (677-21-4) → 1,2,2-trichloro-3,3,3-trifluoropropane (7125-83-9) + 2-chloro-1,1,1-trifluoropropene (2730-62-3) + 2,3-dichloro-1,1,1-trifluoropropane (338-75-0) + (Z)-1-chloro-3,3,3-trifluoro-1-propene (99728-16-2) + 2,3,3,3-tetrafluoro-propene (754-12-1) + 2-chloro-1,3,3,3-tetrafluoropropane (117970-90-8) + trans-1-chloro-3,3,3-trifluoropropene (102687-65-0)

Guidance literature:

With hydrogen fluoride; chlorine; at 140 ℃; Gas phase;

Reference yield:

1,1,1-trifluoropropylene (677-21-4) → 1,2,2-trichloro-3,3,3-trifluoropropane (7125-83-9) + 2-chloro-1,1,1-trifluoropropene (2730-62-3) + 2,3-dichloro-1,1,1-trifluoropropane (338-75-0) + (Z)-1-chloro-3,3,3-trifluoro-1-propene (99728-16-2) + 2,3,3,3-tetrafluoro-propene (754-12-1) + cis-1,2-dichloro-3,3,3-trifluoropropene (25062-10-6) + trans-1,2-dichloro-3,3,3-trifluoropropene (25062-11-7) + 2-chloro-1,3,3,3-tetrafluoropropane (117970-90-8) + trans-1-chloro-3,3,3-trifluoropropene (102687-65-0)

Guidance literature:

With hydrogen fluoride; chlorine; at 140 ℃; Gas phase;

upstream raw materials:

1,1,1-trifluoropropylene

acrylic acid

1,1,1,2,3-pentachloro-propane

2,3-dichloro-1,1,1-trifluoropropane

Downstream raw materials:

1,3,3,3-tetrafluoro-propene

Refernces

• 1、 -. "Compositions". Paragraph 0106; 0107. . Retrieved 2013/09/12.
• 2、 -. "PROCESSES FOR THE PRODUCTION OF FLUOROPROPANES AND HALOPROPENES AND AZEOTROPIC COMPOSITIONS OF 2-CHLORO-3,3,3-TRIFLUORO-1-PROPENE WITH HF AND OF 1,1,1,2,2-PENTAFLUOROPROPANE WITH HF". Page/Page column 18-19. . Retrieved 2008/12/05.