Technology Process of Methanediol, 1-[2-(acetyloxy)-5-aminophenyl]-, 1,1-diacetate
There total 3 articles about Methanediol, 1-[2-(acetyloxy)-5-aminophenyl]-, 1,1-diacetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol;
for 4h;
under 2327.17 Torr;
DOI:10.1002/ejic.200300959
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid / 1 h / 20 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 1140.08 Torr
With
sulfuric acid; hydrogen;
palladium 10% on activated carbon;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: polyphosphoric acid / 1 h / 100 °C
2: sulfuric acid / 1 h / 20 °C
3: hydrogen / palladium 10% on activated carbon / methanol / 1140.08 Torr
With
sulfuric acid; hydrogen;
palladium 10% on activated carbon;
In
methanol;
