methyldi-n-butoxyborane

Base Information Edit

Chemical Name:methyldi-n-butoxyborane
CAS No.:86595-28-0
Molecular Formula:C₉H₂₁BO₂
Molecular Weight:172.076
Hs Code.:
Mol file:86595-28-0.mol

Synonyms:methyldi-n-butoxyborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyldi-n-butoxyborane Edit

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Technology Process of methyldi-n-butoxyborane

There total 2 articles about methyldi-n-butoxyborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 688-74-4
boric acid tributyl ester

: 823-96-1
Trimethylboroxine

: 101-36-0
tri-n-butoxyboroxin

: 86595-28-0
methyldi-n-butoxyborane

Guidance literature:: In tetrahydrofuran; for 0.5h;

Reference yield:

: 688-74-4
boric acid tributyl ester

: 917-54-4
methyllithium

: (CH₃)2B(OC₄H₉)

: 593-90-8
trimethylborane

: 86595-28-0
methyldi-n-butoxyborane

Guidance literature:: With hydrogenchloride; In diethyl ether; under N2; to cold (-78 °C) soln. of boron compd. in Et2O slowly added MeLi, stirred for 0.5 h, warmed to room temp., stirred for 0.5 h,Li(BMe4) detected by (11)B NMR, cooled to 0 °C, added soln. of HCl in Et2O, stirred for 15 min, warmed; not isolated, monitored by (11)B NMR;
DOI:10.1021/om50004a009