2-vinyloxybenzoic acid p-hydroxyanilide

Base Information

• Chemical Name: 2-vinyloxybenzoic acid p-hydroxyanilide
• CAS No.: 86269-47-8
• Molecular Formula: C₁₅H₁₃NO₃
• Molecular Weight: 255.273
• Mol file: 86269-47-8.mol

Synonyms:2-vinyloxybenzoic acid p-hydroxyanilide

Chemical Property of 2-vinyloxybenzoic acid p-hydroxyanilide

Chemical Property:

Purity/Quality:

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Technology Process of 2-vinyloxybenzoic acid p-hydroxyanilide

There total 2 articles about 2-vinyloxybenzoic acid p-hydroxyanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.7%

2-hydroxy-N-(4-hydroxyphenyl)benzamide (526-18-1) + acetylene (74-86-2,25067-58-7) → 2-vinyloxybenzoic acid p-hydroxyanilide (86269-47-8) + 2-hydroxybenzoic acid p-vinyloxyanilide (86269-44-5)

Guidance literature:

potassium hydroxide; In benzene; at 195 - 200 ℃; for 1.5h; under 8360 - 9120 Torr;

DOI:10.1007/BF00516203

Reference yield:

4-amino-phenol (123-30-8) + 2-vinyloxyphenyl benzoate → 2-vinyloxybenzoic acid p-hydroxyanilide (86269-47-8)

Guidance literature:

In ethanol; at 200 - 210 ℃; for 14h; ampul;

DOI:10.1007/BF00516203

upstream raw materials:

4-amino-phenol

2-hydroxy-N-(4-hydroxyphenyl)benzamide

acetylene

Refernces