triethoxy(3-ethoxypropyl)silane

Base Information

• Chemical Name: triethoxy(3-ethoxypropyl)silane
• CAS No.: 81518-55-0
• Molecular Formula: C₁₁H₂₆O₄Si
• Molecular Weight: 250.411
• Mol file: 81518-55-0.mol

Synonyms:triethoxy(3-ethoxypropyl)silane

Chemical Property of triethoxy(3-ethoxypropyl)silane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of triethoxy(3-ethoxypropyl)silane

There total 3 articles about triethoxy(3-ethoxypropyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-ethoxyprop-1-ene (557-31-3) + Triethoxysilane (998-30-1) → ethylpropylether (628-32-0) + triethoxy(3-ethoxypropyl)silane (81518-55-0)

Guidance literature:

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In 5,5-dimethyl-1,3-cyclohexadiene; at 70 ℃; for 12h; Inert atmosphere;

DOI:10.1002/pola.28924

Reference yield:

3-ethoxyprop-1-ene (557-31-3) + Triethoxysilane (998-30-1) → ethylpropylether (628-32-0) + ethyl 1-propenyl ether (928-55-2) + triethoxy(3-ethoxypropyl)silane (81518-55-0)

Guidance literature:

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In 5,5-dimethyl-1,3-cyclohexadiene; diethylene glycol dimethyl ether; at 70 ℃; for 12h; Inert atmosphere;

DOI:10.1002/pola.28924

Reference yield:

3-ethoxyprop-1-ene (557-31-3) + Triethoxysilane (998-30-1) → tetraethoxy orthosilicate (78-10-4) + triethoxy(3-ethoxypropyl)silane (81518-55-0)

Guidance literature:

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In toluene; at 40 - 60 ℃; for 16h; Overall yield = 90 %Spectr.;

DOI:10.1016/j.jcat.2012.06.006

upstream raw materials:

3-ethoxyprop-1-ene

Triethoxysilane

Refernces

• 1、 Gigler, Peter,Drees, Markus,Riener, Korbinian,Bechlars, Bettina,Herrmann, Wolfgang A.,Kuehn, Fritz E.. "Mechanistic insights into the hydrosilylation of allyl compounds - Evidence for different coexisting reaction pathways". . p. 1 - 14. Retrieved 2013/01/14.