methyl 4-isopropoxy-2-methoxymethyloxybenzoate

Base Information

• Chemical Name: methyl 4-isopropoxy-2-methoxymethyloxybenzoate
• CAS No.: 1165713-09-6
• Molecular Formula: C₁₃H₁₈O₅
• Molecular Weight: 254.283
• Mol file: 1165713-09-6.mol

Synonyms:methyl 4-isopropoxy-2-methoxymethyloxybenzoate

Chemical Property of methyl 4-isopropoxy-2-methoxymethyloxybenzoate

Chemical Property:

Purity/Quality:

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Technology Process of methyl 4-isopropoxy-2-methoxymethyloxybenzoate

There total 1 articles about methyl 4-isopropoxy-2-methoxymethyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyl 2-hydroxy-4-isopropyl benzoate (163618-93-7) → methyl 4-isopropoxy-2-methoxymethyloxybenzoate (1165713-09-6)

Guidance literature:

methyl 2-hydroxy-4-isopropyl benzoate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

methoxymethyl halide; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

DOI:10.1016/j.tet.2009.03.089

Reference yield: 95.0%

methyl 4-isopropoxy-2-methoxymethyloxybenzoate (1165713-09-6) → methyl 2-hydroxy-4-isopropyl benzoate (163618-93-7)

Guidance literature:

With silica-immobilized p-TsOH; In toluene; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2009.03.089

Reference yield: 90.0%

methyl 4-isopropoxy-2-methoxymethyloxybenzoate (1165713-09-6) → bis-(methyl-2-hydroxy-4-isopropoxybenzo-5-yl)methane (1165713-54-1) + methyl 2-hydroxy-4-isopropyl benzoate (163618-93-7)

Guidance literature:

With amberlyst-15; In toluene; at 20 ℃; for 0.83h;

DOI:10.1016/j.tet.2009.03.089

upstream raw materials:

methyl 2-hydroxy-4-isopropyl benzoate

Downstream raw materials:

bis-(methyl-2-hydroxy-4-isopropoxybenzo-5-yl)methane

methyl 2-hydroxy-4-isopropyl benzoate

Refernces