4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester)

Base Information

• Chemical Name: 4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester)
• CAS No.: 287737-92-2
• Molecular Formula: C₁₃H₁₉BrO₃S
• Molecular Weight: 335.262
• Mol file: 287737-92-2.mol

Synonyms:4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester)

Chemical Property of 4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester)

There total 2 articles about 4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4-dimethyl-pentan-2-one (590-50-1) → 4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester) (287737-92-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium borate; diethyl ether

With sodium borate; diethyl ether;

DOI:10.1021/ja01618a055

Reference yield:

4.4-Dimethyl-2-pentanol (6144-93-0) + 4-bromobenzenesulfonyl chloride (98-58-8) → 4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester) (287737-92-2)

Guidance literature:

DOI:10.1021/ja01618a055

Reference yield:

4-bromo-benzenesulfonic acid-(1,3,3-trimethyl-butyl ester) (287737-92-2) → (E)-4,4-dimethyl-2-pentene (690-08-4)

Guidance literature:

With potassium acetate; acetic anhydride; acetic acid;

DOI:10.1021/ja01618a055

upstream raw materials:

4.4-Dimethyl-2-pentanol

4-bromobenzenesulfonyl chloride

4,4-dimethyl-pentan-2-one

Downstream raw materials:

(E)-4,4-dimethyl-2-pentene

4,4-dimethylpent-1-ene