DIISOBUTYLAMINE HYDROCHLORIDE

Base Information

• Chemical Name: DIISOBUTYLAMINE HYDROCHLORIDE
• CAS No.: 18251-82-6
• Molecular Formula: C8H19 N . Cl H
• Molecular Weight: 165.706
• Hs Code.: 2921199090
• Mol file: 18251-82-6.mol

Synonyms:1-Propanamine,2-methyl-N-(2-methylpropyl)-, hydrochloride (9CI); Diisobutylamine, hydrochloride(8CI); 2-Methyl-N-(2-methylpropyl)-1-propanamine hydrochloride;Bis(isobutyl)ammonium chloride; Diisobutyl ammonium chloride;N-Isobutyl-2-methylpropylamine hydrochloride

Chemical Property of DIISOBUTYLAMINE HYDROCHLORIDE

Chemical Property:

• Vapor Pressure: 6.12mmHg at 25°C
• Melting Point: 260-265 °C
• Boiling Point: 140.5°C at 760 mmHg
• Flash Point: 29.4°C
• PSA: 12.03000
• LogP: 3.08090
• Water Solubility.: almost transparency

Purity/Quality:

98% ^*data from raw suppliers

Diisobutylamine Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIISOBUTYLAMINE HYDROCHLORIDE

There total 6 articles about DIISOBUTYLAMINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diisobutylamine (110-96-3) → diisobutylamine hydrochloride (18251-82-6)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 2h; Reflux;

DOI:10.1080/00397911.2015.1096943

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + triisobutylamine (1116-40-1) → diisobutylamine hydrochloride (18251-82-6) + isobutene (115-11-7,15220-85-6)

Guidance literature:

at 200 - 210 ℃;

Reference yield:

triisobutylamine (1116-40-1) + isobutyryl chloride (513-36-0) → diisobutylamine hydrochloride (18251-82-6) + isobutene (115-11-7,15220-85-6)

Guidance literature:

upstream raw materials:

triisobutylamine

isobutyryl chloride

diisobutylamine

N-(pentafluorophenyl)carbonimidoyl dichloride

Downstream raw materials:

N,N-diisobutyl-glycine nitrile

N,N-diisobutyl urea

chloro-diisobutyl-amine

N-Nitroso-diisobutylamin

Refernces

• 1、 Di Grandi, Martin J.,Bennett, Caitlin,Cagino, Kristen,Muccini, Arnold,Suraci, Corey,Saba, Shahrokh. "Direct Preparation of Amides from Amine Hydrochloride Salts and Orthoesters: A Synthetic and Mechanistic Perspective". supporting information. p. 2601 - 2607. Retrieved 2015/11/28.