Cyclohexyltrimethoxysilane

Base Information

• Chemical Name: Cyclohexyltrimethoxysilane
• CAS No.: 17865-54-2
• Molecular Formula: C9H20O3Si
• Molecular Weight: 204.341
• Hs Code.: 29319000
• DSSTox Substance ID: DTXSID20451277
• Nikkaji Number: J2.101.254H
• Wikidata: Q72460164
• Mol file: 17865-54-2.mol

Synonyms:Cyclohexyltrimethoxysilane;17865-54-2;cyclohexyl(trimethoxy)silane;Silane, cyclohexyltrimethoxy-;cyclohexyl trimethoxysilane;MFCD01074466;Cyclohexane, (trimethoxysilyl)-;C9H20O3Si;SCHEMBL93335;97%;DTXSID20451277;AMY42240;AKOS015840732;DS-9574;SY041917;C2280;CS-0150973;FT-0693178;FT-0699773;I11386;A881380

Chemical Property of Cyclohexyltrimethoxysilane

Chemical Property:

• Vapor Pressure: 0.199mmHg at 25°C
• Melting Point: <0°C
• Refractive Index: 1.433
• Boiling Point: 217.029 °C at 760 mmHg
• Flash Point: 83.586 °C
• PSA: 27.69000
• Density: 0.955 g/cm³
• LogP: 2.19880
• Storage Temp.: Inert atmosphere,Room Temperature
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 204.11817103
• Heavy Atom Count: 13
• Complexity: 134

Purity/Quality:

98%,99%, ^*data from raw suppliers

Cyclohexyltrimethoxysilane ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CO[Si](C1CCCCC1)(OC)OC

Technology Process of Cyclohexyltrimethoxysilane

There total 5 articles about Cyclohexyltrimethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

methanol (67-56-1) + cyclohexyltrichlorosilane (98-12-4) → cyclohexyl trimethoxysilane (17865-54-2)

Guidance literature:

With pyridine; In pentane; at 0 - 20 ℃; Inert atmosphere; Autoclave;

DOI:10.15227/orgsyn.094.0016

Reference yield: 91.0%

→ cyclohexyl trimethoxysilane (17865-54-2)

Guidance literature:

Reference yield: 73.0%

trimethoxysilane (2487-90-3) + cyclohexene (110-83-8) → cyclohexyl trimethoxysilane (17865-54-2)

Guidance literature:

In tetrahydrofuran; at 50 ℃; for 12h; Reagent/catalyst; Temperature;

upstream raw materials:

methanol

cyclohexyltrichlorosilane

tetramethylorthosilicate

1-bromocyclohexane

Downstream raw materials:

dicyclohexylsilane

tricyclohexylsilane

Refernces

• 1、 -. "METHOD FOR PRODUCING ORGANOSILICON COMPOUND HAVING CYCLIC ALKYL GROUP". Paragraph 0022; 0025; 0028; 0029; 0030; 0031; 0034. . Retrieved 2019/01/06.
• 2、 -. "Process for preparing low-chloride or chloride-free alkoxysilanes". . . Retrieved 2008/06/13.