1-amino-2-trifluoromethylpyridinium mesitylenesulfonate

Base Information

• Chemical Name: 1-amino-2-trifluoromethylpyridinium mesitylenesulfonate
• CAS No.: 895636-79-0
• Molecular Formula: C₆H₆F₃N₂*C₉H₁₁O₃S
• Molecular Weight: 362.373
• Mol file: 895636-79-0.mol

Synonyms:1-amino-2-trifluoromethylpyridinium mesitylenesulfonate

Chemical Property of 1-amino-2-trifluoromethylpyridinium mesitylenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-amino-2-trifluoromethylpyridinium mesitylenesulfonate

There total 1 articles about 1-amino-2-trifluoromethylpyridinium mesitylenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(trifluoromethyl)pyridine (368-48-9) + mesitylenesulfonylhydroxylamine (36016-40-7) → 1-amino-2-trifluoromethylpyridinium mesitylenesulfonate (895636-79-0)

Guidance literature:

In chloroform; at 20 ℃; for 108h;

Reference yield: 60.0%

N-{3-[(2-methylthio-4-pyrimidinyl)ethynyl]phenyl}-2,6-difluorobenzamide (895636-77-8) + 1-amino-2-trifluoromethylpyridinium mesitylenesulfonate (895636-79-0) → N-{3-[3-(2-methyl-4-pyrimidinyl)-7-trifluoromethylpyrazolo[1,5-a]pyridin-2-yl]phenyl}-2,6-difluorobenzamide (895636-80-3)

Guidance literature:

With potassium hydroxide; potassium carbonate; In dimethyl sulfoxide; for 3h;

upstream raw materials:

2-(trifluoromethyl)pyridine

mesitylenesulfonylhydroxylamine

Downstream raw materials:

N-{3-[3-(2-methyl-4-pyrimidinyl)-7-trifluoromethylpyrazolo[1,5-a]pyridin-2-yl]phenyl}-2,6-difluorobenzamide

Refernces