N,N-DIPHENYL-4-METHOXYBENZAMIDE

Base Information

• Chemical Name: N,N-DIPHENYL-4-METHOXYBENZAMIDE
• CAS No.: 16034-40-5
• Molecular Formula: C20H17NO2
• Molecular Weight: 303.36
• Hs Code.: 2924299090
• Mol file: 16034-40-5.mol

Synonyms:4-Methoxy-N,N-diphenylbenzamide;p-Anisamide,N,N-diphenyl- (7CI,8CI);N,N-Diphenyl-p-methoxybenzamide;

Chemical Property of N,N-DIPHENYL-4-METHOXYBENZAMIDE

Chemical Property:

• Vapor Pressure: 6.11E-09mmHg at 25°C
• Melting Point: 140 °C
• Refractive Index: 1.633
• Boiling Point: 468.2 °C at 760 mmHg
• Flash Point: 237 °C
• PSA: 29.54000
• Density: 1.178 g/cm³
• LogP: 4.67370
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N-Diphenyl-4-methoxybenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-DIPHENYL-4-METHOXYBENZAMIDE

There total 9 articles about N,N-DIPHENYL-4-METHOXYBENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-methoxy-benzoyl chloride (100-07-2) + diphenylamine (122-39-4) → N-(4-Methoxybenzoyl)-diphenylamine (16034-40-5)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1021/ja077463q

Reference yield: 99.0%

→ N-(4-Methoxybenzoyl)-diphenylamine (16034-40-5)

Guidance literature:

Reference yield: 93.0%

iodobenzene (591-50-4) + 4-methoxy-N-phenylbenzamide (7465-88-5) → N-(4-Methoxybenzoyl)-diphenylamine (16034-40-5)

Guidance literature:

With potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene; at 130 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol200750p

upstream raw materials:

4-methoxy-N-phenyl-benzimidic acid phenyl ester

4-methoxy-benzoyl chloride

diphenylamine

isocyanate de chlorosulfonyle

Downstream raw materials:

N-(4-methoxybenzyl)-N,N-diphenylamine

(3,4-Dimethoxy-phenyl)-(4-phenylamino-phenyl)-methanone

(3-Nitro-phenyl)-(4-phenylamino-phenyl)-methanone

9-(3-Nitrobenzoyl)-acridine

Refernces

• 1、 Racine, Emilie,Monnier, Florian,Vors, Jean-Pierre,Taillefer, Marc. "A simple copper-catalyzed synthesis of tertiary acyclic amides". supporting information; experimental part. p. 2818 - 2821. Retrieved 2011/07/09.
• 2、 -. "NUCLEAR RECEPTOR BINDING AGENTS". Page/Page column 135-137. . Retrieved 2008/06/13.