CH₃OC₆H₄CHCHBHN(CH(CH₃)2)2

Base Information

• Chemical Name: CH₃OC₆H₄CHCHBHN(CH(CH₃)2)2
• CAS No.: 858347-31-6
• Molecular Formula: C₁₅H₂₄BNO
• Molecular Weight: 245.173
• Mol file: 858347-31-6.mol

Synonyms:CH₃OC₆H₄CHCHBHN(CH(CH₃)2)2

Chemical Property of CH₃OC₆H₄CHCHBHN(CH(CH₃)2)2

Chemical Property:

Purity/Quality:

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Technology Process of CH₃OC₆H₄CHCHBHN(CH(CH₃)2)2

There total 2 articles about CH₃OC₆H₄CHCHBHN(CH(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(Z)-1-bromo-2-(4-methoxyphenyl)ethene (6303-59-9,27570-08-7,60592-52-1) + diisopropopylaminoborane (22092-92-8) → CH3OC6H4CHCHBHN(CH(CH3)2)2 (858347-31-6)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; 80°C, 15 h;

DOI:10.1016/j.jorganchem.2005.01.054

Reference yield: 34.0%

(E)-4-(2-bromo-vinyl)-anisole (6303-59-9,60592-52-1,27570-08-7) + diisopropopylaminoborane (22092-92-8) → CH3OC6H4CHCHBHN(CH(CH3)2)2 (858347-31-6)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; 80°C, 15 h;

DOI:10.1016/j.jorganchem.2005.01.054

upstream raw materials:

(Z)-1-bromo-2-(4-methoxyphenyl)ethene

diisopropopylaminoborane

(E)-4-(2-bromo-vinyl)-anisole

Refernces