1-bromo-6-iodohexane

Base Information

• Chemical Name: 1-bromo-6-iodohexane
• CAS No.: 155345-54-3
• Molecular Formula: C₆H₁₂BrI
• Molecular Weight: 290.97
• Mol file: 155345-54-3.mol

Synonyms:1-bromo-6-iodohexane

Chemical Property of 1-bromo-6-iodohexane

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-bromo-6-iodohexane

There total 1 articles about 1-bromo-6-iodohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1 ,6-dibromohexane (629-03-8) → 1,6-diiodohexane (629-09-4) + 1-bromo-6-iodohexane (155345-54-3)

Guidance literature:

With 1-cetyl-4-aza-1-azonia bicyclo[2.2.2]octane chloride; potassium iodide; In chloroform; water; at 58 ℃; for 24h;

DOI:10.1016/j.tet.2005.03.087

Reference yield: 72.0%

1-bromo-6-iodohexane (155345-54-3) → 1,2-dithiacyclooctane (6008-69-1)

Guidance literature:

With benzyltriethylammonium tetrathiomolybdate; In chloroform; at 28 ℃; for 3h;

Reference yield: 68.0%

C18H20BrNOZn + 1-bromo-6-iodohexane (155345-54-3) → C24H32BrNO

Guidance literature:

With (1,2-dimethoxyethane)dichloronickel(II); 1,5-bis-(diphenylphosphino)pentane; C₁₇H₂₀N₂O; In tetrahydrofuran; at -5 ℃; stereoselective reaction;

DOI:10.1126/science.aaz3855

upstream raw materials:

1 ,6-dibromohexane

Downstream raw materials:

1,2-dithiacyclooctane

C₅₅H₉₆N₂O₇Si₂

C₆₂H₁₀₁BrN₂O₆Si₂

C₇₄H₁₁₃N₃O₇Si₂

Refernces