C₃₈H₆₀N₆O₁₀

Base Information

• Chemical Name: C₃₈H₆₀N₆O₁₀
• CAS No.: 913263-73-7
• Molecular Formula: C₃₈H₆₀N₆O₁₀
• Molecular Weight: 760.929
• Mol file: 913263-73-7.mol

Synonyms:C₃₈H₆₀N₆O₁₀

Chemical Property of C₃₈H₆₀N₆O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₆₀N₆O₁₀

There total 1 articles about C₃₈H₆₀N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + Fmoc-Val-OH (68858-20-8) + N-(9-Fluorenylmethoxycarbonyl)-D-alloisoleucine (118904-37-3,251316-98-0) + (2R,3R)-2-N-(9-fluorenylmethyloxycarbonyl)-D-allothreonine (130674-54-3) + N-(9-fluorenylmethoxycarbonyl)-D-valine (84624-17-9) → C38H60N6O10 (913263-73-7)

Guidance literature:

Multistep reaction.;

DOI:10.1021/jo060976f

Reference yield:

C38H60N6O10 (913263-73-7) → C38H58N6O9

Guidance literature:

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 25 ℃; for 1h;

DOI:10.1021/jo060976f

Reference yield:

C38H60N6O10 (913263-73-7) → C33H50N6O7 (868547-00-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-hydroxybenzotriazole; ethyldiisopropylamine; N,N'-diisopropylcarbodiimide / CH₂Cl₂; dimethylformamide / 1 h / 25 °C

2: 50.2 mg / trifluoroacetic acid / H₂O / 1 h / 25 °C

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/jo060976f

upstream raw materials:

di-tert-butyl dicarbonate

Fmoc-Val-OH

N-(9-Fluorenylmethoxycarbonyl)-D-alloisoleucine

(2R,3R)-2-N-(9-fluorenylmethyloxycarbonyl)-D-allothreonine

Downstream raw materials:

C₃₃H₅₀N₆O₇

Refernces