Technology Process of C12H25N3
There total 7 articles about C12H25N3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 20 - 75 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate; potassium iodide / 1-methyl-pyrrolidin-2-one / 24 h / 80 °C
2.1: hydrogenchloride; water / 2 h / 60 °C
3.1: tetrahydrofuran / 1 h / 50 °C
3.2: 2 h / 20 °C
4.1: hydrogen / palladium on carbon / methanol / 5 h / 20 °C / 2585.81 Torr
5.1: triethylamine / N,N-dimethyl-formamide
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 75 °C / Inert atmosphere
With
hydrogenchloride; lithium aluminium tetrahydride; water; hydrogen; potassium carbonate; triethylamine; potassium iodide;
palladium on carbon;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 1 h / 50 °C
1.2: 2 h / 20 °C
2.1: hydrogen / palladium on carbon / methanol / 5 h / 20 °C / 2585.81 Torr
3.1: triethylamine / N,N-dimethyl-formamide
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 - 75 °C / Inert atmosphere
With
lithium aluminium tetrahydride; hydrogen; triethylamine;
palladium on carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
