1-BUTENE-4,4,4-D3

Base Information

• Chemical Name: 1-BUTENE-4,4,4-D3
• CAS No.: 23086-03-5
• Molecular Formula: C4H5 D3
• Molecular Weight: 59.0837
• Mol file: 23086-03-5.mol

Synonyms:4,4,4-Trideuterio-1-butene

Chemical Property of 1-BUTENE-4,4,4-D3

Chemical Property:

• PSA: 0.00000
• LogP: 1.58240

Purity/Quality:

1-Butene-4,4,4-d3(gas) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-BUTENE-4,4,4-D3

There total 2 articles about 1-BUTENE-4,4,4-D3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C(2)H3CH2CH(C2H5)CH2NH2 → 1-butylene (106-98-9,9003-28-5) + 1-butene-d3 (23086-03-5)

Guidance literature:

With iron pentacarbonyl; Product distribution; Irradiation;

DOI:10.1002/hlca.19890720402

Reference yield:

Pent-1-en-4,4,5,5,5-d5 (80820-43-5) → 1-butene-d3 (23086-03-5) + methane-d3 (676-80-2) + 3-deuteriopropene (1117-89-1) + 1,1-dideuterio-buta-1,3-diene (40529-13-3)

Guidance literature:

In dichloromethane; at 630 ℃; under 225.02 Torr; Product distribution; Thermodynamic data; Kinetics; deuterium distribution; E_A, pyrolysis reaction at different temperatures, radical isomerisation (Retro-en reaction);

upstream raw materials:

Pent-1-en-4,4,5,5,5-d5

Refernces

• 1、 Kopinke, F.-D.,Bach, G.,Ondruschka, B.,Zimmermann, G.. "On the Pyrolysis of Pent-1-ene-4,4,5,5,5-d5". . p. 699 - 707. Retrieved 2007/10/02.