Technology Process of C24H33N3O8
There total 7 articles about C24H33N3O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium tert-butylate / tetrahydrofuran / 20 °C
1.2: 20 °C
2.1: pyridine / dichloromethane / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C
3.2: 1 h / 20 °C
4.1: hydrogen / 5%-palladium/activated carbon / ethanol / 2 h
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 1 h / 20 °C
With
pyridine; potassium tert-butylate; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
5%-palladium/activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dmap / acetonitrile / 0 - 20 °C
2: water; sodium hydroxide / ethanol / 0.5 h / 20 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 1 h / 20 °C
With
water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide;
dmap;
In
tetrahydrofuran; ethanol; acetonitrile;