2-Naphthalenepropanol

Base Information

• Chemical Name: 2-Naphthalenepropanol
• CAS No.: 27650-98-2
• Molecular Formula: C13H14 O
• Molecular Weight: 186.254
• Hs Code.: 2906299090
• DSSTox Substance ID: DTXSID20458680
• Nikkaji Number: J1.520.007C
• Wikidata: Q82282154
• Mol file: 27650-98-2.mol

Synonyms:2-Naphthalenepropanol;27650-98-2;3-naphthalen-2-ylpropan-1-ol;3-(2-naphthyl)-1-propanol;3-(2-naphthyl)propanol;SCHEMBL81147;3-(2-naphtyl)propan-1-ol;3-(2-naphthyl)propan-1-ol;3-(2-naphthyl)-propan-1-ol;DTXSID20458680;HMVMFGNKDHVMJV-UHFFFAOYSA-N;AKOS006288599;3-(NAPHTHALEN-2-YL)PROPAN-1-OL;FT-0724198;EN300-1853411

Chemical Property of 2-Naphthalenepropanol

Chemical Property:

• Melting Point: 41.2-41.4 °C
• Boiling Point: 120-121 °C(Press: 7 Torr)
• PKA: 15.06±0.10(Predicted)
• PSA: 20.23000
• Density: 1.093±0.06 g/cm3(Predicted)
• LogP: 2.76470
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 186.104465066
• Heavy Atom Count: 14
• Complexity: 167

Purity/Quality:

97% ^*data from raw suppliers

3-NAPHTHALEN-2-YL-PROPAN-1-OL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C=C(C=CC2=C1)CCCO

Technology Process of 2-Naphthalenepropanol

There total 2 articles about 2-Naphthalenepropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ α-naphthol (90-15-3) + 2-allyl-1-naphthol (28164-58-1) + 3-(2-naphthyl)propan-1-ol (27650-98-2) + ((E)-2-Propenyl)-naphthalen-1-ol (128113-45-1)

Guidance literature:

In water; acetonitrile; for 1h; Further byproducts given. Title compound not separated from byproducts; Irradiation;

DOI:10.1021/jo00301a030

Reference yield:

trimethylene oxide (503-30-0) + 2-naphthalenylmagnesium bromide (21473-01-8) → 3-(2-naphthyl)propan-1-ol (27650-98-2)

Guidance literature:

With diethyl ether;

DOI:10.1021/ja01145a045

Reference yield: 88.0%

3-(2-naphthyl)propan-1-ol (27650-98-2) → 3-(naphthalen-2-yl)propanal (136415-67-3)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h; Concentration; Time;

upstream raw materials:

trimethylene oxide

2-naphthalenylmagnesium bromide

Downstream raw materials:

3-(naphthalen-2-yl)propanal

naphthalene-2-carboxylate

Refernces