2-(2,6-Dichlorophenoxy)ethylhydrazine

Base Information

• Chemical Name: 2-(2,6-Dichlorophenoxy)ethylhydrazine
• CAS No.: 2347-81-1
• Molecular Formula: C8H10 Cl2 N2 O
• Molecular Weight: 221.086
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID20396578
• Wikidata: Q82197359
• Mol file: 2347-81-1.mol

Synonyms:2-(2,6-dichlorophenoxy)ethylhydrazine;2347-81-1;DTXSID20396578

Chemical Property of 2-(2,6-Dichlorophenoxy)ethylhydrazine

Chemical Property:

• Boiling Point: 370.5±32.0 °C(Predicted)
• PKA: 6.98±0.70(Predicted)
• PSA: 47.28000
• Density: 1.329±0.06 g/cm3(Predicted)
• LogP: 2.92670
• XLogP3: 2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 220.0170183
• Heavy Atom Count: 13
• Complexity: 138

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1)Cl)OCCNN)Cl

Technology Process of 2-(2,6-Dichlorophenoxy)ethylhydrazine

There total 2 articles about 2-(2,6-Dichlorophenoxy)ethylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-bromoethoxy)-1,3-dichlorobenzene (26583-73-3) → 2-(2,6-Dichlorphenoxy)-ethylhydrazin (2347-81-1)

Guidance literature:

With hydrazine hydrate; In ethanol; Heating;

DOI:10.1021/jm00327a029

Reference yield:

→ 2-(2,6-Dichlorphenoxy)-ethylhydrazin (2347-81-1)

Guidance literature:

entspr. Bromverb., N2H4*H2O;

Reference yield: 4.0%

2-(2,6-Dichlorphenoxy)-ethylhydrazin (2347-81-1) + dimethyl N-cyanodithioiminocarbonate (10191-60-3) → 1-<2-(2,6-dichlorophenoxy)-ethyl>-3-methylthio-5-amino-2H-1,2,4-triazole (84827-91-8) + 1-<2-(2,6-dichlorophenoxy)-ethyl>-3-methylthio-5-amino-1H-1,2,4-triazole (84827-90-7)

Guidance literature:

In benzene; at 35 ℃; for 5h;

upstream raw materials:

2-(2-bromoethoxy)-1,3-dichlorobenzene

Downstream raw materials:

guanoclor

1-<2-(2,6-dichlorophenoxy)-ethyl>-3-methylthio-5-amino-2H-1,2,4-triazole

1-<2-(2,6-dichlorophenoxy)-ethyl>-3-methylthio-5-amino-1H-1,2,4-triazole

{2-[2-(2,6-Dichloro-phenoxy)-ethyl]-5-methylsulfanyl-2H-[1,2,4]triazol-3-yl}-[1-phenyl-meth-(Z)-ylidene]-amine

Refernces