histidinylleucinato^(2-)-O,N,N-diphenyltin(IV)

Base Information

• Chemical Name: histidinylleucinato^(2-)-O,N,N-diphenyltin(IV)
• CAS No.: 1093075-61-6
• Molecular Formula: C₂₄H₂₈N₄O₃Sn
• Molecular Weight: 539.221
• Mol file: 1093075-61-6.mol

Synonyms:histidinylleucinato^(2-)-O,N,N-diphenyltin(IV)

Chemical Property of histidinylleucinato^(2-)-O,N,N-diphenyltin(IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of histidinylleucinato^(2-)-O,N,N-diphenyltin(IV)

There total 1 articles about histidinylleucinato^(2-)-O,N,N-diphenyltin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

diphenyltin(IV) dichloride (1135-99-5) + histidinylleucine (7763-65-7,70626-52-7,77327-85-6) → histidinylleucinato(2-)-O,N,N-diphenyltin(IV) (1093075-61-6)

Guidance literature:

With NaOCH₃; In methanol; byproducts: NaCl, methanol; (N2); addn. of methanolic soln. of peptide deriv. to methanolic soln. ofsodium methylate, stirring at room temp. for 0.5 h. refluxing for 4.5-6 .5 h, addn. of hot methanolic soln. of tin compd., refluxing for 14-16 h; centrifugation, filtration, evapn., recrystn. (methanol/hexane or petroleum ether (1:3)), elem. anal.;

DOI:10.1016/j.saa.2008.01.006

upstream raw materials:

diphenyltin(IV) dichloride

histidinylleucine

Refernces