N-(4-nitrobenzyl)-N-nitrosoacetamide

Base Information Edit

Chemical Name:N-(4-nitrobenzyl)-N-nitrosoacetamide
CAS No.:183156-73-2
Molecular Formula:C₉H₉N₃O₄
Molecular Weight:223.188
Hs Code.:
Mol file:183156-73-2.mol

Synonyms:N-(4-nitrobenzyl)-N-nitrosoacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-nitrobenzyl)-N-nitrosoacetamide Edit

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Technology Process of N-(4-nitrobenzyl)-N-nitrosoacetamide

There total 2 articles about N-(4-nitrobenzyl)-N-nitrosoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 56222-10-7
N-(4-nitrobenzyl)acetamide

: 183156-73-2
N-(4-nitrobenzyl)-N-nitrosoacetamide

Guidance literature:: With sodium acetate; dinitrogen tetraoxide; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo990494m

Reference yield:

: 7409-30-5
p-nitrobenzylamine

: 183156-73-2
N-(4-nitrobenzyl)-N-nitrosoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / diethyl ether / 1.08 h / 25 °C

2: 100 percent / NaOAc; N₂O₄ / CH₂Cl₂ / 1 h / 0 °C

With sodium acetate; dinitrogen tetraoxide; In diethyl ether; dichloromethane; 1: Acetylation / 2: Nitrosation;
DOI:10.1021/jo990494m