C₈H₅ClF₈OS

Base Information

• Chemical Name: C₈H₅ClF₈OS
• CAS No.: 1594970-70-3
• Molecular Formula: C₈H₅ClF₈OS
• Molecular Weight: 336.633
• Mol file: 1594970-70-3.mol

Synonyms:C₈H₅ClF₈OS

Chemical Property of C₈H₅ClF₈OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₈H₅ClF₈OS

There total 4 articles about C₈H₅ClF₈OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(1,2,2-trifluorovinyloxy)benzene (772-53-2) → C8H5ClF8OS (1594970-70-3)

Guidance literature:

With pentafluorosulfanyl chloride; dibenzoyl peroxide; at 20 - 110 ℃; for 8h; Temperature; Inert atmosphere;

DOI:10.1021/ol500766v

Reference yield:

phenol (108-95-2,27073-41-2) → C8H5ClF8OS (1594970-70-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium hydroxide; tetrabutylammomium bromide / 4 - 10 °C

2.1: potassium hydroxide / methanol / Inert atmosphere

2.2: 250 - 280 °C / Inert atmosphere

3.1: dibenzoyl peroxide; pentafluorosulfanyl chloride / 8 h / 20 - 110 °C / Inert atmosphere

With pentafluorosulfanyl chloride; tetrabutylammomium bromide; potassium hydroxide; dibenzoyl peroxide; In methanol;

DOI:10.1021/ol500766v

Reference yield:

potassium phenolate (100-67-4) → C8H5ClF8OS (1594970-70-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 °C / Autoclave; Inert atmosphere

2: 240 - 260 °C / Inert atmosphere; Pyrolysis

3: dibenzoyl peroxide; pentafluorosulfanyl chloride / 8 h / 20 - 110 °C / Inert atmosphere

With pentafluorosulfanyl chloride; dibenzoyl peroxide;

DOI:10.1021/ol500766v

upstream raw materials:

(1,2,2-trifluorovinyloxy)benzene

phenol

potassium phenolate

C₉H₅F₄O₃^(1-)*K⁽¹⁺⁾

Refernces