1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine

Base Information Edit

Chemical Name:1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine
CAS No.:137116-92-8
Molecular Formula:C₂₂H₂₀N₂
Molecular Weight:312.414
Hs Code.:
Mol file:137116-92-8.mol

Synonyms:1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine Edit

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Technology Process of 1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine

There total 6 articles about 1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 583-11-9,59130-82-4
N-(1-phenylethylidene)phenylhydrazine

: 137116-92-8
1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In toluene; at 80 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.6b00702

Reference yield: 53.0%

: 23686-03-5
1,3,6-triphenyl-1,4-dihydro-pyridazine

: 137116-92-8
1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 15200 Torr; Ambient temperature;

Reference yield:

: 98-86-2
acetophenone

: 137116-92-8
1,3,6-triphenyl-1,4,5,6-tetrahydropyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / Reflux; Inert atmosphere

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / toluene / 80 °C / Inert atmosphere; Schlenk technique

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; acetic acid; In ethanol; toluene;
DOI:10.1021/acs.orglett.6b00702