4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride

Base Information

• Chemical Name: 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride
• CAS No.: 60007-31-0
• Molecular Formula: C₁₇H₁₁ClN₂O
• Molecular Weight: 294.74
• Mol file: 60007-31-0.mol

Synonyms:4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride

Chemical Property of 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride

Chemical Property:

Purity/Quality:

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Technology Process of 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride

There total 1 articles about 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,6-diphenyl-2-pyrimidinecarboxylic acid (6483-96-1) → 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride (60007-31-0)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In benzene; for 24h; Heating;

DOI:10.1007/BF00515002

Reference yield: 80.0%

1-amino-3-methylbenzene (108-44-1) + 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride (60007-31-0) → 4,6-diphenyl-pyrimidine-2-carboxylic acid m-tolylamide

Guidance literature:

With pyridine; In benzene; for 5h; Heating;

DOI:10.1007/BF02508412

Reference yield: 77.0%

thiosemicarbazide (79-19-6) + 4,6-diphenyl-2-pyrimidinecarboxylic acid chloroanhydride (60007-31-0) → 1-(4,6-Diphenyl-pyrimidin-2-oyl)thiosemicarbazid (203789-54-2)

Guidance literature:

With sodium hydrogencarbonate; In 1,4-dioxane; for 3h; Ambient temperature;

upstream raw materials:

4,6-diphenyl-2-pyrimidinecarboxylic acid

Downstream raw materials:

p-Cyanophenyl 4,6-Diphenylpyrimidine-2-carboxylate

1-(4,6-Diphenyl-pyrimidin-2-oyl)thiosemicarbazid

Refernces