4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde

Base Information

• Chemical Name: 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde
• CAS No.: 92498-33-4
• Molecular Formula: C₁₅H₁₁NO₆
• Molecular Weight: 301.255
• Mol file: 92498-33-4.mol

Synonyms:4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde

Chemical Property of 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde

There total 5 articles about 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-fluoro-3-nitrobenzaldehyde (42564-51-2) + vanillin (121-33-5,8014-42-4) → 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde (92498-33-4)

Guidance literature:

With tetrabutyl-ammonium chloride; potassium carbonate; for 0.0833333h; microwave irradiation;

DOI:10.1016/S0957-4166(02)00742-5

Reference yield:

4-hydroxy-3-nitrobenzaldehyde (3011-34-5) → 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde (92498-33-4)

Guidance literature:

Multi-step reaction with 2 steps

2: pyridine

With pyridine;

DOI:10.1139/v58-236

Reference yield:

3-nitro-4-(toluene-4-sulfonyloxy)-benzaldehyde (107559-00-2) + vanillin (121-33-5,8014-42-4) → 4-(4-formyl-2-methoxyphenoxy)-3-nitrobenzaldehyde (92498-33-4)

Guidance literature:

With pyridine;

DOI:10.1139/v58-236

upstream raw materials:

3-nitro-4-(toluene-4-sulfonyloxy)-benzaldehyde

vanillin

4-chloro-3-nitro-benzaldehyde

4-fluoro-3-nitrobenzaldehyde

Downstream raw materials:

(2-nitro-2'-methoxy-4,4'-di(2-ethoxycarbonylethenyl))diphenyl ether

(2-hydroxy-2'-methoxy-4,4'-di(2-ethoxycarbonylethenyl))diphenyl ether

(2,2'-dimethoxy-4,4'-di(2-ethoxycarbonylethenyl))diphenyl ether

(2-amino-2'-methoxy-4,4'-di(2-ethoxycarbonylethenyl))diphenyl ether

Refernces