5-(4-chlorophenoxy)acenaphthenequinone

Base Information

• Chemical Name: 5-(4-chlorophenoxy)acenaphthenequinone
• CAS No.: 1422531-71-2
• Molecular Formula: C₁₈H₉ClO₃
• Molecular Weight: 308.721
• Mol file: 1422531-71-2.mol

Synonyms:5-(4-chlorophenoxy)acenaphthenequinone

Chemical Property of 5-(4-chlorophenoxy)acenaphthenequinone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(4-chlorophenoxy)acenaphthenequinone

There total 2 articles about 5-(4-chlorophenoxy)acenaphthenequinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

5-bromoacenaphthylene-1,2-dione (26254-35-3) + 4-chloro-phenol (106-48-9,82344-39-6) → 5-(4-chlorophenoxy)acenaphthenequinone (1422531-71-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 4h;

DOI:10.1016/j.ejmech.2012.10.050

Reference yield:

acenaphthene quinone (82-86-0) → 5-(4-chlorophenoxy)acenaphthenequinone (1422531-71-2)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / 60 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

With bromine; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.10.050

upstream raw materials:

5-bromoacenaphthylene-1,2-dione

4-chloro-phenol

acenaphthene quinone

Refernces