methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate

Base Information

• Chemical Name: methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate
• CAS No.: 1013632-22-8
• Molecular Formula: C₁₉H₂₃NO₂S₂
• Molecular Weight: 361.529
• Mol file: 1013632-22-8.mol

Synonyms:methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate

Chemical Property of methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate

Chemical Property:

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Technology Process of methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate

There total 1 articles about methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl hydroxy(phenyl)carbamodithioate (1013632-21-7) + 1-Adamantanecarbonyl chloride (2094-72-6) → methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate (1013632-22-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; Darkness;

DOI:10.1021/ol702832x

Reference yield: 82.0%

methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate (1013632-22-8) → 1-adamantyl methyl phenylcarbonimidodithioate (1013632-26-2)

Guidance literature:

In dichloromethane; at 5 ℃; for 2h; Sunlight irradiation;

DOI:10.1021/ol702832x

Reference yield: 67.0%

methyl 1-adamantylcarbonyloxy(phenyl)carbamodithioate (1013632-22-8) → 1-Azidoadamantane (24886-73-5) + 1-adamantyl methyl phenylcarbonimidodithioate (1013632-26-2)

Guidance literature:

With phenylsulfonyl azide; In dichloromethane; at 5 ℃; for 4h; Sunlight irradiation;

DOI:10.1021/ol702832x

upstream raw materials:

methyl hydroxy(phenyl)carbamodithioate

1-Adamantanecarbonyl chloride

Downstream raw materials:

1-adamantyl methyl phenylcarbonimidodithioate

1-Azidoadamantane

Refernces