Carbamodithioic acid, (3-aminopropyl)methyl- (9CI)

Base Information

• Chemical Name: Carbamodithioic acid, (3-aminopropyl)methyl- (9CI)
• CAS No.: 343926-83-0
• Molecular Formula: C5H12 N2 S2
• Molecular Weight: 164.296
• Mol file: 343926-83-0.mol

Synonyms:Carbamodithioic acid, (3-aminopropyl)methyl- (9CI)

Chemical Property of Carbamodithioic acid, (3-aminopropyl)methyl- (9CI)

Chemical Property:

• PSA: 100.15000
• LogP: 1.18200

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamodithioic acid, (3-aminopropyl)methyl- (9CI)

There total 1 articles about Carbamodithioic acid, (3-aminopropyl)methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + N-Methyl-1,3-propanediamine (6291-84-5) → (3-Amino-propyl)-methyl-dithiocarbamic acid (343926-83-0)

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1021/jm00141a015

Reference yield:

(3-Amino-propyl)-methyl-dithiocarbamic acid (343926-83-0) → tetrahydro-1-methyl-1H-pyrimidine-2-thione (24421-05-4)

Guidance literature:

With hydrogenchloride; In ethanol; for 10h; Yield given; Heating;

DOI:10.1021/jm00141a015

Reference yield:

(3-Amino-propyl)-methyl-dithiocarbamic acid (343926-83-0) → 1-methyltetrahydropyrimidin-2(1H)-one (10166-54-8)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / aq. ethanol / 10 h / Heating

2: 61 percent / 30percent H₂O₂, 10percent aq. NaOH / 0.5 h / 70 °C

With hydrogenchloride; sodium hydroxide; dihydrogen peroxide; In ethanol;

DOI:10.1021/jm00141a015

upstream raw materials:

carbon disulfide

N-Methyl-1,3-propanediamine

Downstream raw materials:

tetrahydro-1-methyl-1H-pyrimidine-2-thione

1-methyltetrahydropyrimidin-2(1H)-one

Refernces