O-acetyl S,S-diethyl phosphorodithioite

Base Information

• Chemical Name: O-acetyl S,S-diethyl phosphorodithioite
• CAS No.: 84103-76-4
• Molecular Formula: C₆H₁₃O₂PS₂
• Molecular Weight: 212.274
• Mol file: 84103-76-4.mol

Synonyms:O-acetyl S,S-diethyl phosphorodithioite

Chemical Property of O-acetyl S,S-diethyl phosphorodithioite

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of O-acetyl S,S-diethyl phosphorodithioite

There total 2 articles about O-acetyl S,S-diethyl phosphorodithioite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

S,S-diethyl-N-diethylamidodithiophosphite (42964-63-6) + acetic anhydride (108-24-7) → diethylacetamide (685-91-6) + O-acetyl S,S-diethyl phosphorodithioite (84103-76-4)

Guidance literature:

for 20h; Product distribution; Ambient temperature;

Reference yield: 83.0%

S,S-diethyl-N-diethylamidodithiophosphite (42964-63-6) + acetic acid (64-19-7,77671-22-8) → N,N-diethylamine acetate (20726-63-0) + O-acetyl S,S-diethyl phosphorodithioite (84103-76-4)

Guidance literature:

for 1h; Ambient temperature;

Reference yield: 89.0%

O-acetyl S,S-diethyl phosphorodithioite (84103-76-4) → diethyl phosphorochloridodithioite (1486-42-6) + acetic anhydride (108-24-7)

Guidance literature:

With acetyl chloride; for 0.5h; Ambient temperature;

upstream raw materials:

S,S-diethyl-N-diethylamidodithiophosphite

acetic anhydride

acetic acid

Downstream raw materials:

S,S-diethyldithiophosphorous acid methyl ester

acetic acid

ethyl thioacetate

diethyl phosphorochloridodithioite

Refernces

• 1、 Sinyashin, O. G.,Kostin, V. P.,Batyeva, E. S.,Pudovik, A. N.. "ACIDOLYSIS OF DIALKYL PHOSPHORAMIDODITHIOITES. O-ACETYL PHOSPHORODITHIOITES". . p. 2382 - 2384. Retrieved 2007/10/02.