PHENYL METHICONE

Base Information

• Chemical Name: PHENYL METHICONE
• CAS No.: 31230-04-3
• Molecular Formula: C₇H₁₀O₂Si
• Molecular Weight: 154.241
• Mol file: 31230-04-3.mol

Synonyms:Silanediol,methylphenyl-, homopolymer (9CI); Silanediol, methylphenyl-, polymers (8CI);Methylphenylsilanediol homopolymer; Methylphenylsilanediol polymer;Poly(methylphenylsilanediol); Poly(methylphenylsiloxane);Polyphenylmethylsiloxane

Chemical Property of PHENYL METHICONE

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of PHENYL METHICONE

There total 9 articles about PHENYL METHICONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

dimethoxy(methyl)phenylsilane (3027-21-2) → methyl(phenyl)silanediol (3959-13-5,31230-04-3)

Guidance literature:

With water; In acetonitrile; at 25 ℃; for 0.0833333h;

Reference yield: 99.0%

methylphenylsilane (766-08-5,146088-00-8) → methyl(phenyl)silanediol (3959-13-5,31230-04-3)

Guidance literature:

With oxygen; In water; acetone; at 30 ℃; for 0.333333h; under 760.051 Torr;

DOI:10.1246/cl.150379

Reference yield: 81.0%

bis(2-thienyl)methylphenylsilane (31650-28-9) → methyl(phenyl)silanediol (3959-13-5,31230-04-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1016/j.tetlet.2006.03.095

upstream raw materials:

Dichloromethylsilane

diethoxy-methyl-phenyl-silane

dichloromethylphenylsilane

dimethoxy(methyl)phenylsilane

Downstream raw materials:

C₁₅H₂₈Cl₂O₆Si₃

2,2,6,6-Tetraethoxy-4,8-dimethyl-4,8-diphenyl-[1,3,5,7,2,4,6,8]tetroxatetrasilocane

C₂₉H₃₆Cl₆O₆Si₇

4-(4-tolyl)anisole

Refernces

• 1、 Kannengie?er, Jan-Falk,Briesenick, Max,Meier, Dennis,Huch, Volker,Morgenstern, Bernd,Kickelbick, Guido. "Synthesis and Hydrogen-Bond Patterns of Aryl-Group Substituted Silanediols and -triols from Alkoxy- and Chlorosilanes". . p. 16461 - 16476. Retrieved 2021/10/25.
• 2、 Nakamura, Masaharu,Matsumoto, Yotaro,Toyama, Masaaki,Baba, Masanori,Hashimoto, Yuichi. "Organosilicon compounds as adult T-cell leukemia cell proliferation inhibitors". . p. 237 - 241. Retrieved 2013/03/14.