tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate

Base Information

• Chemical Name: tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate
• CAS No.: 128408-43-5
• Molecular Formula: C₁₈H₂₂O₈
• Molecular Weight: 366.368
• Mol file: 128408-43-5.mol

Synonyms:tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate

Chemical Property of tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate

There total 1 articles about tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

dimethyl acetylenedicarboxylate (762-42-5) + hex-1-yne (693-02-7) → hexamethyl benzenehexacarboxylate (6237-59-8) + tetramethyl 5-(n-butyl)-1,2,3,4-benzenetetracarboxylate (128408-43-5)

Guidance literature:

With 1,2-bis-(diphenylphosphino)ethane; bis(1,5-cyclooctadiene)diiridium(I) dichloride; In toluene; for 1h; Heating;

DOI:10.1021/ol035330d

upstream raw materials:

dimethyl acetylenedicarboxylate

hex-1-yne

Refernces

• 1、 Dieck, Heindirk tom,Munz, Christina,Mueller, Christiane. "Diazadienes as control ligands in homogeneous catalysis XVIII. Palladacyclopentadienes and platinacyclopentadienes and the co-cyclotrimerization of various alkynes". . p. 243 - 255. Retrieved 2007/10/02.