Technology Process of methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate
There total 11 articles about methyl 2-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
1,4-dioxane;
for 4h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
1,4-dioxane;
at 120 ℃;
for 3h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ja503163k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: [tris(2,4-di-tert-butylphenyl)phosphine]gold chloride; silver hexafluoroantimonate / dichloromethane / 0.02 h / 20 °C / Inert atmosphere
2: triethylamine; dmap / dichloromethane / 0.25 h / 0 - 20 °C / Inert atmosphere
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 3 h / 120 °C / Inert atmosphere; Sealed tube
With
dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; silver hexafluoroantimonate; [tris(2,4-di-tert-butylphenyl)phosphine]gold chloride; potassium acetate; triethylamine;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/ja503163k