dioxorhenium(VII) tris(fluorosulfate)

Base Information

• Chemical Name: dioxorhenium(VII) tris(fluorosulfate)
• CAS No.: 97295-57-3
• Molecular Formula: 3FO₃S*O₂Re
• Molecular Weight: 515.394
• Mol file: 97295-57-3.mol

Synonyms:dioxorhenium(VII) tris(fluorosulfate)

Chemical Property of dioxorhenium(VII) tris(fluorosulfate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of dioxorhenium(VII) tris(fluorosulfate)

There total 3 articles about dioxorhenium(VII) tris(fluorosulfate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rhenium + bis(fluorosulfuryl) peroxide (13709-32-5) + fluorosulphonic acid (7789-21-1) → dioxorhenium(VII) tris(fluorosulfate) (97295-57-3)

Guidance literature:

In fluorosulphonic acid; HSO3F is distd. onto Re, FSO2OOSO2F is added in vac., heated to 80°C for 12 d; removing of all volatile material;

Reference yield:

bis(fluorosulfuryl) peroxide (13709-32-5) + rhenium(VII) oxide → dioxorhenium(VII) tris(fluorosulfate) (97295-57-3)

Guidance literature:

byproducts: O2; FSO2OOSO2F is distd. in vac. onto Re2O7, heated for 48 h at 80°C; excess peroxide is removed in vac., elem. anal.;

Reference yield:

rhenium + bis(fluorosulfuryl) peroxide (13709-32-5) → dioxorhenium(VII) tris(fluorosulfate) (97295-57-3)

Guidance literature:

FSO2OOSO2F is added to Re, heated to 80°C for 48 h;

upstream raw materials:

bis(fluorosulfuryl) peroxide

fluorosulphonic acid

Refernces