2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester

Base Information

• Chemical Name: 2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester
• CAS No.: 145372-04-9
• Molecular Formula: C₃₀H₃₀O₆
• Molecular Weight: 486.565
• Mol file: 145372-04-9.mol

Synonyms:2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester

Chemical Property of 2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester

There total 1 articles about 2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

butyl 3-hydroxynaphthalene-2-carboxylate (7260-07-3) + β-naphthol (135-19-3) → Butyl 2,2'-dihydroxy-1,1'-binaphthalene-3-carboxylate (145372-03-8) + 2,2'-Dihydroxy-[1,1']binaphthalenyl-3,3'-dicarboxylic acid dibutyl ester (145372-04-9) + 1,1'-bi-2-naphthol (602-09-5)

Guidance literature:

With tert-butylamine; copper dichloride; In isopropyl alcohol; at 50 ℃; for 2h; Yields of byproduct given;

DOI:10.1016/S0040-4020(01)88318-6

upstream raw materials:

butyl 3-hydroxynaphthalene-2-carboxylate

β-naphthol

Refernces