C₄₁H₆₁NO₄

Base Information

• Chemical Name: C₄₁H₆₁NO₄
• CAS No.: 1350449-24-9
• Molecular Formula: C₄₁H₆₁NO₄
• Molecular Weight: 631.94
• Mol file: 1350449-24-9.mol

Synonyms:C₄₁H₆₁NO₄

Chemical Property of C₄₁H₆₁NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₁H₆₁NO₄

There total 4 articles about C₄₁H₆₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-4-(1,1-dimethylethyl)pyridine (81167-60-4) → C41H61NO4 (1350449-24-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: dihydrogen peroxide; acetic acid / water / Reflux

2.1: trichlorophosphate / Reflux; Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 - 20 °C / Inert atmosphere

3.2: 0.5 h / Inert atmosphere

3.3: 16 h / 75 °C / Inert atmosphere

With dihydrogen peroxide; tert.-butyl lithium; acetic acid; trichlorophosphate; In tetrahydrofuran; water; pentane;

DOI:10.1021/om201069k

Reference yield:

4-tert-butylpyridine (3978-81-2) → C41H61NO4 (1350449-24-9)

Guidance literature:

Multi-step reaction with 5 steps

1.1: dihydrogen peroxide; acetic acid / water / Reflux

2.1: trichlorophosphate / Reflux; Inert atmosphere

3.1: dihydrogen peroxide; acetic acid / water / Reflux

4.1: trichlorophosphate / Reflux; Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 - 20 °C / Inert atmosphere

5.2: 0.5 h / Inert atmosphere

5.3: 16 h / 75 °C / Inert atmosphere

With dihydrogen peroxide; tert.-butyl lithium; acetic acid; trichlorophosphate; In tetrahydrofuran; water; pentane;

DOI:10.1021/om201069k

Reference yield:

4-tert-butylpyridine N-oxide (23569-17-7) → C41H61NO4 (1350449-24-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: trichlorophosphate / Reflux; Inert atmosphere

2.1: dihydrogen peroxide; acetic acid / water / Reflux

3.1: trichlorophosphate / Reflux; Inert atmosphere

4.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 - 20 °C / Inert atmosphere

4.2: 0.5 h / Inert atmosphere

4.3: 16 h / 75 °C / Inert atmosphere

With dihydrogen peroxide; tert.-butyl lithium; acetic acid; trichlorophosphate; In tetrahydrofuran; water; pentane;

DOI:10.1021/om201069k

upstream raw materials:

4-tert-butylpyridine

4-tert-butylpyridine N-oxide

4-tert-butyl-2-chloro-1-oxidopyridin-1-ium

2-chloro-4-(1,1-dimethylethyl)pyridine

Downstream raw materials:

4-tert-butylpyridine-2,6-bis[2-(4,6-di-tert-butylphenol)]

Refernces