Technology Process of 2,4-bis(benzyloxy)-6-pentadecanylbenzoic acid
There total 6 articles about 2,4-bis(benzyloxy)-6-pentadecanylbenzoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
water; dimethyl sulfoxide;
at 90 ℃;
for 24h;
DOI:10.1021/jo051384k
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 4.15 g / NaH2PO4; NaClO2 / dimethylsulfoxide; H2O / 20 °C
2.1: 99 percent / DBU / acetonitrile / 20 °C
3.1: LDA / tetrahydrofuran; hexane / 0.33 h / -78 °C
3.2: 70 percent / tetrahydrofuran; hexane / -78 - 20 °C
4.1: 82 percent / BBr3 / CH2Cl2 / 48 h / -10 °C
5.1: K2CO3 / acetone / 12 h / Heating
6.1: 1.40 g / KOH / dimethylsulfoxide; H2O / 24 h / 90 °C
With
potassium hydroxide; sodium chlorite; sodium dihydrogenphosphate; boron tribromide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; acetonitrile;
DOI:10.1021/jo051384k
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 99 percent / DBU / acetonitrile / 20 °C
2.1: LDA / tetrahydrofuran; hexane / 0.33 h / -78 °C
2.2: 70 percent / tetrahydrofuran; hexane / -78 - 20 °C
3.1: 82 percent / BBr3 / CH2Cl2 / 48 h / -10 °C
4.1: K2CO3 / acetone / 12 h / Heating
5.1: 1.40 g / KOH / dimethylsulfoxide; H2O / 24 h / 90 °C
With
potassium hydroxide; boron tribromide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium diisopropyl amide;
In
tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; acetone; acetonitrile;
DOI:10.1021/jo051384k
