benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate

Base Information

• Chemical Name: benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate
• CAS No.: 1069131-25-4
• Molecular Formula: C₁₆H₂₁NO₂
• Molecular Weight: 259.348
• Mol file: 1069131-25-4.mol

Synonyms:benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate

Chemical Property of benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate

Chemical Property:

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Technology Process of benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate

There total 1 articles about benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2-(2-methylenecyclopentyl)ethanamine + benzyl chloroformate (501-53-1,94274-21-2) → benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate (1069131-25-4)

Guidance literature:

With triethylamine; In diethyl ether; ethanol; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo801631v

Reference yield: 79.0%

benzyl 2-(2-methylidenecyclopentyl)ethylcarbamate (1069131-25-4) + 1-bromo-3,5-dichlorobenzene (19752-55-7) → (+/-)-(3aR,6aS)-benzyl 6a-(3,5-dichlorobenzyl)hexahydrocyclopenta[b]pyrrole-1(2H)-carboxylate

Guidance literature:

With palladium diacetate; caesium carbonate; nixantphos; In 1,4-dioxane; at 100 ℃; for 20h; Inert atmosphere;

DOI:10.1021/jo801631v

upstream raw materials:

benzyl chloroformate

Refernces