dimethyl-amine; compound with boron chloride

Base Information

• Chemical Name: dimethyl-amine; compound with boron chloride
• CAS No.: 856314-21-1
• Molecular Formula: BCl₃*C₂H₇N
• Molecular Weight: 162.254
• Mol file: 856314-21-1.mol

Synonyms:dimethyl-amine; compound with boron chloride

Chemical Property of dimethyl-amine; compound with boron chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of dimethyl-amine; compound with boron chloride

There total 1 articles about dimethyl-amine; compound with boron chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethylchloroamine (1585-74-6) + diboron tetrachloride (13701-67-2) → boron trichloride (10294-34-5) + dimethyl-amine; compound with boron chloride (856314-21-1)

Guidance literature:

In neat (no solvent); under N2, with exclusion of moisture, reagents (1/1 mol ratio) gently warmed to room temp.; not sepd.; detected by NMR, IR;

Reference yield:

dimethyl-amine; compound with boron chloride (856314-21-1) + dimethyl amine (124-40-3) → dichlorodimethylaminoborane (1113-31-1) + chloro-bis(dimethylamino)borane (6562-41-0) + tris(diethylamino)borane (867-97-0) + N,N-dimethylammonium chloride (506-59-2)

Guidance literature:

with NHMe2 excess;

upstream raw materials:

dimethylchloroamine

diboron tetrachloride

Downstream raw materials:

dichlorodimethylaminoborane

chloro-bis(dimethylamino)borane

tris(diethylamino)borane

N,N-dimethylammonium chloride

Refernces