Technology Process of C30H22ClNO3
There total 7 articles about C30H22ClNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H19NO2;
With
potassium tert-butylate;
In
tetrahydrofuran;
at -40 ℃;
for 1h;
4-chloro-benzoyl chloride;
In
tetrahydrofuran;
for 3h;
DOI:10.1021/jm301084z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene / 12 h
2.1: water; acetonitrile / 5 h / Reflux
3.1: hydrogenchloride; water / 1,4-dioxane / 2 h / Reflux
4.1: caesium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C
5.1: potassium tert-butylate / tetrahydrofuran / 1 h / -40 °C
5.2: 3 h
With
hydrogenchloride; potassium tert-butylate; water; caesium carbonate;
In
tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm301084z
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium hydroxide / methanol / 4 h / Reflux
2.1: dimethyl amine / acetic acid / 3 h / 0 °C / pH 12
3.1: toluene / 12 h
4.1: water; acetonitrile / 5 h / Reflux
5.1: hydrogenchloride; water / 1,4-dioxane / 2 h / Reflux
6.1: caesium carbonate / N,N-dimethyl-formamide / 5 h / 0 - 20 °C
7.1: potassium tert-butylate / tetrahydrofuran / 1 h / -40 °C
7.2: 3 h
With
hydrogenchloride; potassium tert-butylate; water; caesium carbonate; dimethyl amine; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; acetic acid; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jm301084z
