4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde

Base Information

• Chemical Name: 4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde
• CAS No.: 860523-83-7
• Molecular Formula: C₁₄H₁₀I₂O₃
• Molecular Weight: 480.041
• Mol file: 860523-83-7.mol

Synonyms:4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde

Chemical Property of 4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde

There total 2 articles about 4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(3,5-diiodo-4-methoxy-phenoxy)-benzonitrile (855290-86-7) → 4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde (860523-83-7)

Guidance literature:

With hydrogenchloride; chloroform; tin(ll) chloride; Reagens 4: Aether, Erhitzen des Reaktionsprodukts mit wss.HCl;

DOI:10.1577/1548-8659(2000)129<0194:GPSAOO>2.0.CO;2

Reference yield:

4-(3,5-diiodo-4-methoxy-phenoxy)-aniline; hydrochloride → 4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde (860523-83-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid; copper (II)-sulfate; water

2: chloroform; SnCl₂; HCl / Reagens 4: Aether, Erhitzen des Reaktionsprodukts mit wss.HCl

With hydrogenchloride; chloroform; water; copper(II) sulfate; acetic acid; tin(ll) chloride;

DOI:10.1577/1548-8659(2000)129<0194:GPSAOO>2.0.CO;2

Reference yield:

4-(3,5-diiodo-4-methoxy-phenoxy)-benzaldehyde (860523-83-7) → 3',5'-diiodothyronine (60363-25-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate; acetic acid anhydride / Erwaermen des danach isolierten Reaktionsprodukts mit wss.-aethanol. Natronlauge

2: phosphorus; phosphinic acid; aqueous hydriodic acid / anschl. Erhitzen mit wss. Bromwasserstoffsaeure

With phosphorus; hydrogen iodide; sodium acetate; hypophosphorous acid; acetic anhydride;

DOI:10.1577/1548-8659(2000)129<0194:GPSAOO>2.0.CO;2

upstream raw materials:

4-(3,5-diiodo-4-methoxy-phenoxy)-benzonitrile

Downstream raw materials:

3',5'-diiodothyronine