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pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium(0)

Base Information Edit
  • Chemical Name:pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium(0)
  • CAS No.:104267-43-8
  • Molecular Formula:C16H12CrO6
  • Molecular Weight:352.264
  • Hs Code.:
  • Mol file:104267-43-8.mol
pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium<sup>(0)</sup>

Synonyms:pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium(0)

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Chemical Property of pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium(0) Edit
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Technology Process of pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium(0)

There total 3 articles about pentacarbonyl[ethoxy(phenylethenyl)carbene]chromium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In hexane; benzene; soln. of Cr-complex and ligand in hexane-benzene was heated at reflux for 9 h under Ar; solvent was removed under reduced pressure, flash column chromy. (SiO2, hexane-AcOEt); elem. anal.;
DOI:10.1021/om034347x
Guidance literature:
With triethylamine; In diethyl ether; byproducts: Et3N*HCl, Me3SiOSiMe3; under Ar, dissolving of aldehyde, Et3N, Me3SiCl and Cr-complex at 25°C for 4 days;; detn. of react. endpoint by DC, evapn., dissolving of residue with toluene, column chromy. (Kieselgel, petroleum ether), elem. anal.;;
Guidance literature:
In Petroleum ether; heating at 25°C in a small amount of petroleum ether;;
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