Technology Process of dimethyl(phenyl)gallium
There total 3 articles about dimethyl(phenyl)gallium which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
hexane;
to a supsn. of (C6H5)3Ga in n-hexane was added through a syringe (CH3)3Ga, the soln. was heated at 100°C for 2 h, cooled to room temp.; volatiles were removed under reduced pressure (10 mbar); elem. anal.;
DOI:10.1021/om701055a
- Guidance literature:
-
In
neat (no solvent);
in an Schlenk flask (CH3)3Ga was added to freshly sublimed (C6H5)2Hg, the vessel was tightly closed, the suspn. was heated at 100°C for 5h, cooled to room temp.; volatiles were removed under reduced pressure (10 mbar), the residue waswashed twice with n-hexane at -70°C; elem. anal.;
DOI:10.1021/om701055a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: neat (no solvent)
2: hexane
In
hexane;
DOI:10.1021/om701055a
