Technology Process of 5-(trifluoro-λ4-boraneyl)quinoline potassium salt
There total 6 articles about 5-(trifluoro-λ4-boraneyl)quinoline potassium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
quinolin-5-ylmethanesulfonate;
With
tetrahydroxydiboron; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
ethanol;
at 80 ℃;
for 8h;
Inert atmosphere;
Sealed tube;
With
potassium hydrogen difluoride;
In
methanol; ethanol; water;
at 0 - 20 ℃;
for 0.5h;
DOI:10.1021/jo401104y
- Guidance literature:
-
5-chloroquinoline;
With
tetrahydroxydiboron; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
ethanol;
at 80 ℃;
for 12h;
Inert atmosphere;
Sealed tube;
With
potassium hydrogen difluoride;
In
methanol; ethanol; water;
at 0 - 20 ℃;
for 0.5h;
DOI:10.1021/jo401104y
- Guidance literature:
-
5-bromoquinoline; bis(pinacol)diborane;
With
10H-phenothiazine; caesium carbonate;
In
acetonitrile;
for 18h;
Irradiation;
Sealed tube;
Inert atmosphere;
potassium fluoride;
With
L-Tartaric acid;
In
tetrahydrofuran; methanol; water; acetonitrile;
With
potassium carbonate;
In
acetonitrile;
for 2h;
DOI:10.1021/jacs.9b12519
