Technology Process of 1-chloro-1-methyl-5-phenylpentyl p-tolyl sulfoxide
There total 5 articles about 1-chloro-1-methyl-5-phenylpentyl p-tolyl sulfoxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
Yield given. Multistep reaction;
1.) THF, -65 deg C, 10 min, 2.) THF, from -65 deg C to -35 deg C, 2 h;
DOI:10.1016/0040-4020(95)01078-5
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / tributylphosphine / tetrahydrofuran / a) 0 deg C, 20 min, b) RT, 18 h
2: N-chlorosuccinimide / CCl4 / 2 h / Ambient temperature
3: m-chloroperbenzoic acid / CH2Cl2 / 1 h / -50 °C
4: 1.) LDA / 1.) THF, -65 deg C, 10 min, 2.) THF, from -65 deg C to -35 deg C, 2 h
With
N-chloro-succinimide; tributylphosphine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1016/0040-4020(95)01078-5
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / tributylphosphine / tetrahydrofuran / a) 0 deg C, 20 min, b) RT, 18 h
2: N-chlorosuccinimide / CCl4 / 2 h / Ambient temperature
3: m-chloroperbenzoic acid / CH2Cl2 / 1 h / -50 °C
4: 1.) LDA / 1.) THF, -65 deg C, 10 min, 2.) THF, from -65 deg C to -35 deg C, 2 h
With
N-chloro-succinimide; tributylphosphine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1016/0040-4020(95)01078-5
