C₁₃H₁₆N₄O

Base Information

• Chemical Name: C₁₃H₁₆N₄O
• CAS No.: 1247949-17-2
• Molecular Formula: C₁₃H₁₆N₄O
• Molecular Weight: 244.296
• Mol file: 1247949-17-2.mol

Synonyms:C₁₃H₁₆N₄O

Chemical Property of C₁₃H₁₆N₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₆N₄O

There total 3 articles about C₁₃H₁₆N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(2-ethoxyphenyl)-5-aminopyrazole (1247949-16-1,502132-92-5) + C3H7NO*2ClH → C13H16N4O (1247949-17-2)

Guidance literature:

In methanol; at 20 ℃; for 1h;

Reference yield:

ethyl 2-ethoxybenzoate (6290-24-0) → C13H16N4O (1247949-17-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium tert-butylate / toluene / 1.17 h / 20 °C / Cooling with ice

1.2: pH ~ 1

2.1: hydrazine hydrate / methanol / 2.5 h / Reflux

3.1: methanol / 1 h / 20 °C

With potassium tert-butylate; hydrazine hydrate; In methanol; toluene;

Reference yield:

3-(2-ethoxyphenyl)-3-oxopropanenitrile (89-44-1) → C13H16N4O (1247949-17-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 2.5 h / Reflux

2: methanol / 1 h / 20 °C

With hydrazine hydrate; In methanol;

upstream raw materials:

ethyl 2-ethoxybenzoate

3-(2-ethoxyphenyl)-3-oxopropanenitrile

3-(2-ethoxyphenyl)-5-aminopyrazole

Downstream raw materials:

C₁₃H₁₄N₄O

C₂₅H₃₁N₇O

C₁₄H₁₈N₄O₂

C₂₁H₂₄N₄O₄S

Refernces