o-nitro-N¹-phenylsulfanylamide

Base Information

• Chemical Name: o-nitro-N¹-phenylsulfanylamide
• CAS No.: 19837-88-8
• Molecular Formula: C₁₂H₁₁N₃O₄S
• Molecular Weight: 293.303
• Mol file: 19837-88-8.mol

Synonyms:o-nitro-N¹-phenylsulfanylamide

Chemical Property of o-nitro-N¹-phenylsulfanylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-nitro-N¹-phenylsulfanylamide

There total 6 articles about o-nitro-N¹-phenylsulfanylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-acetyl-sulfanilic acid-(2-nitro-anilide) (7461-20-3) → o-nitro-N1-phenylsulfanylamide (19837-88-8)

Guidance literature:

With hydrogenchloride; ethanol;

Reference yield:

p-acetylaminobenzenesulfonyl chloride (121-60-8) → o-nitro-N1-phenylsulfanylamide (19837-88-8)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone; pyridine

2: hydrogen chloride; ethanol

With pyridine; hydrogenchloride; ethanol; acetone;

Reference yield:

Acetanilid (103-84-4) → o-nitro-N1-phenylsulfanylamide (19837-88-8)

Guidance literature:

Multi-step reaction with 3 steps

1: chlorosulfonic acid / 0.5 h / 60 °C

2: pyridine / 4 h / 0 - 20 °C

3: sodium hydroxide / methanol / 3 h / 70 °C

With pyridine; chlorosulfonic acid; sodium hydroxide; In methanol;

DOI:10.1016/j.ejmech.2020.112890

upstream raw materials:

N-acetyl-sulfanilic acid-(2-nitro-anilide)

2-Chloronitrobenzene

p-acetylaminobenzenesulfonamide

2-nitro-aniline

Downstream raw materials:

dimethyl (2E,4Z)-4-[({4-[(2-nitrophenyl)sulfamoyl]phenyl}amino)methylene]pent-2-enedioate

2-[(2,6-dichlorophenyl)amino]-N₁-(2-nitrophenyl)-N₄-phenylacetoxyacetamidobenzenesulfonamide

Refernces