Bis(11-azidoundecyl) disulfide

Base Information

• Chemical Name: Bis(11-azidoundecyl) disulfide
• CAS No.: 881375-91-3
• Molecular Formula: C₂₂H₄₄N₆S₂
• Molecular Weight: 456.764
• Hs Code.: 2930909090
• Mol file: 881375-91-3.mol

Synonyms:Bis(11-azidoundecyl) disulfide

Chemical Property of Bis(11-azidoundecyl) disulfide

Chemical Property:

• PSA: 150.10000
• LogP: 8.91572
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

Bis(11-azidoundecyl) disulfide 99% (HPLC) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bis(11-azidoundecyl) disulfide

There total 5 articles about Bis(11-azidoundecyl) disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-azido-11-undecanyl 4-methylbenzenesulfonate (833453-13-7) → 1,2-bis(11-azidoundecyl)disulfane (881375-91-3)

Guidance literature:

With thiourea; In ethanol; at 80 ℃; for 12h;

DOI:10.1021/jacs.5b06306

Reference yield: 55.0%

bis(11-methanesulfonate undecanyl)disulfide → 1,2-bis(11-azidoundecyl)disulfane (881375-91-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; for 48h; Inert atmosphere;

DOI:10.1002/adfm.201000729

Reference yield:

11-azidoundecane-1-thiol (668420-70-0) → 1,2-bis(11-azidoundecyl)disulfane (881375-91-3)

Guidance literature:

With iodine; In methanol;

upstream raw materials:

1-Bromo-11-hydroxyundecane

11-azidoundecanol

1-azido-11-undecanyl 4-methylbenzenesulfonate

11-azidoundecane-1-thiol

Refernces

• 1、 Jishkariani, Davit,Diroll, Benjamin T.,Cargnello, Matteo,Klein, Dahlia R.,Hough, Lawrence A.,Murray, Christopher B.,Donnio, Bertrand. "Dendron-Mediated Engineering of Interparticle Separation and Self-Assembly in Dendronized Gold Nanoparticles Superlattices". . p. 10728 - 10734. Retrieved 2015/09/28.