Technology Process of C29H48O4
There total 9 articles about C29H48O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 20 ℃;
for 18h;
DOI:10.1002/ejoc.201402240
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C
1.2: 18 h / 20 °C
2.1: potassium hydroxide / N,N-dimethyl-formamide; water / 4 h / 0 - 20 °C
3.1: pyridine / dichloromethane / 18 h / 0 - 20 °C
4.1: titanium tetrachloride / dichloromethane / 72 h / 0 °C / Reflux
5.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C
With
pyridine; dmap; titanium tetrachloride; sodium hydride; dicyclohexyl-carbodiimide; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
4.1: |Fries Phenol Ester Rearrangement / 5.1: |Steglich Esterification;
DOI:10.1002/ejoc.201402240
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
2: dichloromethane / 5 h / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 20 °C
4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 18 h / 20 °C
With
dmap; palladium 10% on activated carbon; hydrogen; Dess-Martin periodane; dicyclohexyl-carbodiimide;
In
methanol; dichloromethane;
4: |Steglich Esterification;
DOI:10.1002/ejoc.201402240