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C50H75N9O12S

Base Information Edit
  • Chemical Name:C50H75N9O12S
  • CAS No.:111491-74-8
  • Molecular Formula:C50H75N9O12S
  • Molecular Weight:1026.26
  • Hs Code.:
  • Mol file:111491-74-8.mol
C<sub>50</sub>H<sub>75</sub>N<sub>9</sub>O<sub>12</sub>S

Synonyms:C50H75N9O12S

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Chemical Property of C50H75N9O12S Edit
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Technology Process of C50H75N9O12S

There total 12 articles about C50H75N9O12S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; triethylamine; isopentyl nitrite; In 1,4-dioxane; chloroform; N,N-dimethyl-formamide; 1) 0 to 4 deg C, 12 h; 2) 20-25 deg C, 5 h.;
DOI:10.1007/BF00598358
Guidance literature:
Multi-step reaction with 4 steps
1: 1) (CH3)3SiCl; 2) Et3N, pivaloyl chloride / 1) CH2Cl2-DMFA (5:1), 20 min, room temp.; 2) CH2Cl2, -5 deg C, 1 h, 0 deg C, 12 h.
2: 1) (CH3)3SiCl; 2) Et3N, butyl chloroformate / 1) CH2Cl2-DMFA; 2) CH2Cl2.
3: 73 percent / hydrogen, Pd black / methanol / 3 h
4: 76 percent / 1) isoamyl nitrite, Et3N, HCl / dioxane; CHCl3; dimethylformamide / 1) 0 to 4 deg C, 12 h; 2) 20-25 deg C, 5 h.
With hydrogenchloride; chloro-trimethyl-silane; hydrogen; pivaloyl chloride; palladium; triethylamine; carbonochloridic acid, butyl ester; isopentyl nitrite; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1007/BF00598358
Guidance literature:
Multi-step reaction with 4 steps
1: 1) (CH3)3SiCl; 2) Et3N, ethyl chloroformate / 1) CH2Cl2-DMF; 2) CH2Cl2.
2: 1) hydrogen, Pd black, HCl; 2) Et3N, pivaloyl chloride / 1) DMFA, 2) CH2Cl2, 0 to -5 deg C, 12 h.
3: 89 percent / hydrazine hydrate / methanol / 11 h / Ambient temperature
4: 76 percent / 1) isoamyl nitrite, Et3N, HCl / dioxane; CHCl3; dimethylformamide / 1) 0 to 4 deg C, 12 h; 2) 20-25 deg C, 5 h.
With hydrogenchloride; chloro-trimethyl-silane; hydrogen; chloroformic acid ethyl ester; pivaloyl chloride; hydrazine hydrate; palladium; triethylamine; isopentyl nitrite; In 1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1007/BF00598358
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