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methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate

Base Information Edit
  • Chemical Name:methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate
  • CAS No.:1616786-26-5
  • Molecular Formula:C10H13NO3
  • Molecular Weight:195.218
  • Hs Code.:
  • Mol file:1616786-26-5.mol
methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate

Synonyms:methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate

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Chemical Property of methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate Edit
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Technology Process of methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate

There total 3 articles about methyl 2-hydroxy-3-(N,N-dimethylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 2h;
Guidance literature:
methyl 3-(N,N-dimethylamino)benzoate-N-oxide; With trifluoroacetic anhydride; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;
With triethylamine; In dichloromethane; at -78 - 0 ℃; for 0.25h; Overall yield = 38 %; Inert atmosphere;
DOI:10.1021/ol501813s
Guidance literature:
Multi-step reaction with 2 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 23 °C / Inert atmosphere
2.1: trifluoroacetic anhydride / dichloromethane / 1 h / -78 °C / Inert atmosphere
2.2: 0.25 h / -78 - 0 °C / Inert atmosphere
With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1021/ol501813s
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